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      Methods of Gold and Silver Nanoparticles Preparation

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          Abstract

          The versatile family of nanoparticles is considered to have a huge impact on the different fields of materials research, mostly nanoelectronics, catalytic chemistry and in study of cytocompatibility, targeted drug delivery and tissue engineering. Different approaches for nanoparticle preparation have been developed, not only based on “bottom up” and “top down” techniques, but also several procedures of effective nanoparticle modifications have been successfully used. This paper is focused on different techniques of nanoparticles’ preparation, with primary focus on metal nanoparticles. Dispergation methods such as laser ablation and vacuum sputtering are introduced. Condensation methods such as reduction with sodium citrate, the Brust–Schiffrin method and approaches based on ultraviolet light or biosynthesis of silver and gold are also discussed. Basic properties of colloidal solutions are described. Also a historical overview of nanoparticles are briefly introduced together with short introduction to specific properties of nanoparticles and their solutions.

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          Most cited references115

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          A study of the nucleation and growth processes in the synthesis of colloidal gold

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            Does the antibacterial activity of silver nanoparticles depend on the shape of the nanoparticle? A study of the Gram-negative bacterium Escherichia coli.

            In this work we investigated the antibacterial properties of differently shaped silver nanoparticles against the gram-negative bacterium Escherichia coli, both in liquid systems and on agar plates. Energy-filtering transmission electron microscopy images revealed considerable changes in the cell membranes upon treatment, resulting in cell death. Truncated triangular silver nanoplates with a {111} lattice plane as the basal plane displayed the strongest biocidal action, compared with spherical and rod-shaped nanoparticles and with Ag(+) (in the form of AgNO(3)). It is proposed that nanoscale size and the presence of a {111} plane combine to promote this biocidal property. To our knowledge, this is the first comparative study on the bactericidal properties of silver nanoparticles of different shapes, and our results demonstrate that silver nanoparticles undergo a shape-dependent interaction with the gram-negative organism E. coli.
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              Synthesis of thiol-derivatised gold nanoparticles in a two-phase Liquid–Liquid system

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                Author and article information

                Journal
                Materials (Basel)
                Materials (Basel)
                materials
                Materials
                MDPI
                1996-1944
                18 December 2019
                January 2020
                : 13
                : 1
                : 1
                Affiliations
                [1 ]Department of Solid State Engineering, The University of Chemistry and Technology, 166 28 Prague, Czech Republic; nikola.kasalkova@ 123456vscht.cz (N.S.K.); jakub.siegel@ 123456vscht.cz (J.S.); vaclav.svorcik@ 123456vscht.cz (V.Š.)
                [2 ]Faculty of Science, J.E. Purkyně University, 400 96 Ústí nad Labem, Czech Republic
                Author notes
                Article
                materials-13-00001
                10.3390/ma13010001
                6981963
                31861259
                b1fdb2a6-56e0-4fdf-8b23-9e9da7577927
                © 2019 by the authors.

                Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license ( http://creativecommons.org/licenses/by/4.0/).

                History
                : 04 November 2019
                : 13 December 2019
                Categories
                Review

                nanoparticle,preparation,noble metal,surface
                nanoparticle, preparation, noble metal, surface

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