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      Multidisciplinary discovery of ancient restoration using a rare mud carapace on a mummified individual from late New Kingdom Egypt

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          Abstract

          CT scans of an unnamed mummified adult from Egypt, now in the Chau Chak Wing Museum, University of Sydney (NMR.27.3), reveal it to be fully sheathed in a mud shell or carapace, exposing a mortuary treatment not previously documented in the Egyptian archaeological record. The carapace was placed between layers of linen wrappings thus it was not externally visible. Radiocarbon dating of textile samples provide a range of c.1370–1113 cal BC (95.4% probability), with a median date of 1207 cal BC. When assessed against mummification techniques of the era, the individual is placed in the late 19th–20th Dynasty, at the later end of this date range. Multi-proxy analysis including μ-XRF and Raman spectroscopy of carapace fragments from the head area revealed it to consist of three layers, comprising a thin base layer of mud, coated with a white calcite-based pigment and a red-painted surface of mixed composition. Whether the whole surface of the carapace was painted red is unknown. The carapace was a form of ancient conservation applied subsequent to post-mortem damage to the body, intended to reconfigure the body and enable continued existence of the deceased in the afterlife. The carapace can also be interpreted as a form of elite emulation imitating resin shells found within the wrappings of royal bodies from this period.

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          IntCal13 and Marine13 Radiocarbon Age Calibration Curves 0–50,000 Years cal BP

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            Discussion Reporting of 14C Data

            Count rates, representing the rate of 14C decay, are the basic data obtained in a 14C laboratory. The conversion of this information into an age or geochemical parameters appears a simple matter at first. However, the path between counting and suitable 14C data reporting (table 1) causes headaches to many. Minor deflections in pathway, depending on personal interpretations, are possible and give end results that are not always useful for inter-laboratory comparisons. This discussion is an attempt to identify some of these problems and to recommend certain procedures by which reporting ambiguities can be avoided.
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              Methods for Summarizing Radiocarbon Datasets

              Bayesian models have proved very powerful in analyzing large datasets of radiocarbon ( 14 C) measurements from specific sites and in regional cultural or political models. These models require the prior for the underlying processes that are being described to be defined, including the distribution of underlying events. Chronological information is also incorporated into Bayesian models used in DNA research, with the use of Skyline plots to show demographic trends. Despite these advances, there remain difficulties in assessing whether data conform to the assumed underlying models, and in dealing with the type of artifacts seen in Sum plots. In addition, existing methods are not applicable for situations where it is not possible to quantify the underlying process, or where sample selection is thought to have filtered the data in a way that masks the original event distribution. In this paper three different approaches are compared: “Sum” distributions, postulated undated events, and kernel density approaches. Their implementation in the OxCal program is described and their suitability for visualizing the results from chronological and geographic analyses considered for cases with and without useful prior information. The conclusion is that kernel density analysis is a powerful method that could be much more widely applied in a wide range of dating applications.
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                Author and article information

                Contributors
                Role: ConceptualizationRole: Data curationRole: Funding acquisitionRole: InvestigationRole: MethodologyRole: Project administrationRole: SupervisionRole: ValidationRole: VisualizationRole: Writing – original draftRole: Writing – review & editing
                Role: ConceptualizationRole: Formal analysisRole: InvestigationRole: MethodologyRole: SupervisionRole: ValidationRole: VisualizationRole: Writing – original draftRole: Writing – review & editing
                Role: Formal analysisRole: InvestigationRole: ResourcesRole: ValidationRole: VisualizationRole: Writing – original draft
                Role: Formal analysisRole: InvestigationRole: MethodologyRole: ResourcesRole: ValidationRole: VisualizationRole: Writing – original draft
                Role: InvestigationRole: Writing – original draftRole: Writing – review & editing
                Role: Formal analysisRole: Investigation
                Role: Formal analysisRole: Investigation
                Role: Investigation
                Role: Data curationRole: Formal analysisRole: InvestigationRole: ResourcesRole: SoftwareRole: SupervisionRole: ValidationRole: VisualizationRole: Writing – original draft
                Role: Editor
                Journal
                PLoS One
                PLoS One
                plos
                plosone
                PLoS ONE
                Public Library of Science (San Francisco, CA USA )
                1932-6203
                3 February 2021
                2021
                : 16
                : 2
                : e0245247
                Affiliations
                [1 ] Department of History and Archaeology, Macquarie University, Sydney, New South Wales, Australia
                [2 ] McDonald Institute for Archaeological Research, Department of Archaeology, University of Cambridge, Cambridge, United Kingdom
                [3 ] Centre for Accelerator Science, Australian Nuclear Science and Technology Organisation, Sydney, New South Wales, Australia
                [4 ] Department of Earth and Environmental Sciences, Macquarie University, Sydney, New South Wales, Australia
                [5 ] Faculty of Medicine and Health Sciences, Macquarie University, Sydney, New South Wales, Australia
                Hebrew University, ISRAEL
                Author notes

                Competing Interests: The authors have declared that no competing interests exist.

                Author information
                https://orcid.org/0000-0003-4438-9225
                Article
                PONE-D-20-28344
                10.1371/journal.pone.0245247
                7857556
                33534798
                0c1f02f2-006e-4073-8b50-3d35780b6154
                © 2021 Sowada et al

                This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

                History
                : 9 September 2020
                : 23 December 2020
                Page count
                Figures: 7, Tables: 2, Pages: 17
                Funding
                Funded by: funder-id http://dx.doi.org/10.13039/501100001023, Australian Institute of Nuclear Science and Engineering;
                Award ID: AINGRA07/136P
                Award Recipient :
                Funded by: Rundle Foundation for Egyptian Archaeology
                Award Recipient :
                (1) Australian Institute of Nuclear Science and Engineering Grant # AINGRA07/136P URL www.ainse.edu.au The competitive grant covered the cost of radiocarbon dating but did not play any role in the study design, data collection, analysis, decision to publish, or preparation of the manuscript (2) Rundle Foundation for Egyptian Archaeology https://www.mq.edu.au/research/research-centres-groups-and-facilities/resilient-societies/centres/cache/our-projects/the-australian-centre-for-egyptology The competitive grant assisted with preparation of the manuscript, but otherwise did not play any role in the study design, data collection and analysis, or decision to publish.
                Categories
                Research Article
                Research and Analysis Methods
                Imaging Techniques
                Neuroimaging
                Computed Axial Tomography
                Biology and Life Sciences
                Neuroscience
                Neuroimaging
                Computed Axial Tomography
                Medicine and Health Sciences
                Diagnostic Medicine
                Diagnostic Radiology
                Tomography
                Computed Axial Tomography
                Research and Analysis Methods
                Imaging Techniques
                Diagnostic Radiology
                Tomography
                Computed Axial Tomography
                Medicine and Health Sciences
                Radiology and Imaging
                Diagnostic Radiology
                Tomography
                Computed Axial Tomography
                Social Sciences
                Archaeology
                Archaeological Dating
                Radioactive Carbon Dating
                Research and Analysis Methods
                Chemical Characterization
                Isotope Analysis
                Radioactive Carbon Dating
                Physical Sciences
                Materials Science
                Materials
                Pigments
                Earth Sciences
                Mineralogy
                Mud
                Biology and Life Sciences
                Anatomy
                Musculoskeletal System
                Skeleton
                Skull
                Cranium
                Medicine and Health Sciences
                Anatomy
                Musculoskeletal System
                Skeleton
                Skull
                Cranium
                People and Places
                Geographical Locations
                Asia
                Egypt
                People and Places
                Geographical Locations
                Africa
                Egypt
                Social Sciences
                Archaeology
                Archaeological Dating
                Biology and Life Sciences
                Anatomy
                Neck
                Medicine and Health Sciences
                Anatomy
                Neck
                Custom metadata
                All relevant data are within the paper.

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